https://people.chem.umass.edu/mcdaniel/chem269/experiments/aak/procedure.pdf
This is possible by using Hydranal-K reagents since they sufficiently suppress the formation of acetals and ketals. Page 3. Laboratory Report L 676
9 mai 2015 structures and properties of aldehydes and ketones ... Lab Reports: Laboratory reports will consist of three parts: pre-lab questions
With the same reagent aldehydes usually react faster than ketones
25 juil. 2018 Laboratory Report L 676
This reaction consumes water and leads to an erroneously low water content. Water determination in aldehydes and ketones. HYDRANAL™ Laboratory Report L 676.
The chemistry of aldehydes and ketones is characterized by the versatile reactivity of the carbonyl group In this experiment you and a partner will be given an unknown aldehyde and an unknown ketone and you will determine their identities by performing several chemical reactions Oxidation by chromic acid
you will explore the chemical properties of four families of organic compounds aldehydes (RCHO) ketones (R2CO) carboxylic acids (RCOOH) and amines (RNH 2 ) The solubility of each compound in water and hexane will be tested
Aldehydes and Ketones Introduction Aldehydes and ketones share the carbonyl functional group which features carbon doubly bonded to oxygen In the case of ketones there are two carbon atoms bonded to the carbonyl carbon and no hydrogens In the case of aldehydes there is at least one
In an aldehyde one of the bonds on the carbonyl carbon is to a hydrogen atom whereas in ketones both other atoms that are attached to the carbonyl carbon are carbons Because the carbonyl group is present in both aldehydes and ketones the two classes often react similarly
Aldehydes and ketones both contain the C=O or carbonyl group Aldehydes have at least one hydrogen bonded directly to the C=O whereas ketones always have two alkyl groups attached to the C=O OO C RHRR'an aldehydea ketone Because they contain the polar carbonyl group aldehydes and ketones are polar compounds
Ketones and aldehydes both form semicarbazones The melting point of the derivative can be compared to the literature melting points to help identify the compounds Physical Properties of Aldehydes Name bpt ( C) Refractive index (at 20 C) Semicarbazone mpt ( C) 2-furaldehyde 161 1 5260 202 Cyclohexane-carbaldehyde 162 1 4500 173