Laboratory Manual
Experiment 2: Preparation of an azoic dye: Para-red . answers to post-lab questions should be kept in your notebook. The Mechanics of Keeping a Lab ...
Chem 228 FS/2012 Synthesis of Para Red: Library Assignment (due
Oct 17 2012 Synthesis of Para Red: Library Assignment. (due 10/17/12). Name_____________________ ... Attach this Sheet to Your Search Results.
Experiment 8 Synthesis of an Azo Dye - the Coupling Reaction of
Photos of the experiment are available at http://www.chem.cuhk.edu.hk/ssc.htm. 1. Prepare 30 cm3 of ~10% aqueous sodium hydroxide solution by dissolving 3 g of.
Synthesis of Para Red part 1
In this lab you prepare p-nitroaniline by the nitration of acetanilide and diazotize this compound and use the diazonium salt to synthesize the dye.
Format of the Formal Laboratory Report
Aug 19 2010 SAMPLE LAB REPORT ... Synthesis of Benzopinacolone from benzophenone. ... The cork was secured to the test tube using more parafilm and wire ...
Laboratory Solution Preparation
Molarity therefore
A SN1 Reaction: Synthesis of tert-Butyl Chloride
This lab experiment proposes the synthesis of an alkyl halide by reacting the 2 The first report of a 4(3H)-quinazolinone compound: P. Griess J. Prakt.
Synthesis of Para Red part 1 - West Virginia University
Synthesis of Para Red: Dissolve 2 7 g of 2-naphthol in 50 ml of 2 5M NaOH solution Cool the solution to 10 °C by adding crushed ice Carefully pour this solution into the flask containing the remainder of the diazonium salt while swirling Continue to swirl the mixture vigorously for a few minutes then acidify it with 1 M sulfuric acid
EXPERIMENT 6 DYES DYEING PART 1: PREPARATION OF PARA RED AND
Complete the synthesis and purification of para-nitroaniline in Week 6 In Week 7 set up your Grignard reaction at the beginning of your lab section and while refluxing you can begin synthesizing the azo dye which is made from the para-nitroaniline which you synthesized in week 6 All dying will be done Week 7
EXPERIMENT 5 DYES DYEING PART 2: PREPARATION OF PARA RED AND
Pre-lab Questions: 1) Draw the structure of alizarine yellow R (found in section 25 16 in Smith) What starting materials are need to synthesize methyl orange using the same strategy we are using in this experiment (coupling a diazonium salt with a strongly electron-domating aromatic compound)?
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