Supplementary Information Selective monomethylation of primary
Amines are under hydrochloride salt form and the corresponding 1H NMR spectra were recorded in. CD3OD except where indicated. Table 1 (CDCl3
Amine hydrochloride salts: a problem in polyurethane synthesis
The solution phase was investigated using quantitative IH NMR spectroscopy for which a pre-saturation pulse programme had been developed. The proposed reaction
1H and 15N NMR Characterization of the Amine Groups of Heparan
28 mai 2015 amine protons are examined and the possibility of a salt bridge ... Hydrochloric acid (HCl) and dibasic sodium phosphate were.
Supporting Information for: Design Synthesis
http://www.rsc.org/suppdata/gc/c2/c2gc16240g/c2gc16240g.pdf
Transition metal-free catalytic reduction of primary amides using an
Isolated as amine hydrochloride salt. b The yields were determined from 1H NMR spectroscopy using 13
Iron/Caffeine as a Catalytic System for Microwave-Promoted
3 mars 2021 rectly formed from alcohols and amine hydrochloride salts in ... ternal references (CHCl3 ? = 7.26 ppm for 1H NMR and CDCl3
Transition metal-free catalytic reduction of primary amides using an
Isolated as amine hydrochloride salt. b The yields were determined from 1H NMR spectroscopy using 13
Tandem Fe/Zn or Fe/In catalysis for the selective synthesis of
1H NMR spectra were recorded in CDCl3 or d6-DMSO at ambient temperature on Bruker AVANCE to obtain the corresponding amine hydrochloride salt 5.
Transition metal-free catalytic reduction of primary amides using an
26 déc. 2019 Isolated as amine hydrochloride salt. b The yields were determined from 1H NMR spectroscopy using 13
Supporting Information Title: Design and synthesis of selective
N-benzyl-1-(2-(methylamino)ethyl)piperidin-4-amine (5). Benzyl bromide (154 mg 107 ?L) is used. Yield (3x HCl salt): 8% (22 mg) over 4 steps. 1H NMR (600
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