[PDF] Lecture 15: Powder Metallurgy - ektukz





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POWDER METALLURGY • Characterization of Engineering Powders • Production of Metallic Powders • Conventional Pressing and Sintering • Alternative Pressing and Sintering Techniques • Materials and Products for PM • Design Considerations in Powder Metallurgy Dr M Medraj Mech 421/6511 lecture 12/2 Introduction • Feasible when

What is powder metallurgy?

    POWDER METALLURGY (P/M) Feasible when the melting point of a metal is too high such as W, Ta, Mo the reaction occurs when melting such as Zr and for superhard tool materials Powder Metallurgy (PM) (around 1800s)

What are the advantages and disadvantages of powder metallurgy?

    Powder Metallurgy (PM) (around 1800s) Pressing – Powders are compressed into the desired shape in a press-type machine using punch-and-die tooling designed specifically for the part. Sintering - Heating at a temperature well below melting. Advantage Near-net shape, No waste, controlled porosity,Dimension control better than casting Disadvantage

What is the conventional method of compacting metal powders in pm?

    FIGURE 7.4: Pressing, the conventional method of compacting metal powders in PM: (1) filling the die cavity with powder, done by automatic feed in production, (2) initial, and (3) final positions of upper and lower punches during compaction, and (4) ejection of part.

Can powder metallurgy produce more complex parts with true three-dimensional geometries?

    More complex parts with true three-dimensional geometries are also feasible in powder metallurgy, by adding secondary operations such as machining to complete the shape of the pressed and sintered part, and by observing certain design guidelines PRACTICE QUESTIONS 7.1.

NC State University

Department of Materials Science and Engineering 1

MSE 440/540: Processing of Metallic Materials

Instructors: Yuntian Zhu

Office: 308 RBII

Ph : 513-0559 ytzhu@ncsu.edu

Lecture 15: Powder Metallurgy

NC State University

Powder Metallurgy (PM)

Usual PM production sequence:

1. Pressing - powders are compressed into desired shape to produce green compact

Accomplished in press using punch-and-die

2. Sintering - green compacts are heated to bond the particles into a hard, rigid mass

Temperatures are below melting point

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Why Powder Metallurgy is Important

PM parts can be mass produced to net shape or near net shape

PM process wastes very little material - ~ 3%

PM parts can be made with a specified level of porosity, to produce porous metal parts

Filters, oil䇳impregnated bearings and gears

Difficult to fabricate parts can be shaped by powder metallurgy Tungsten filaments for incandescent lamp bulbs are made by PM Certain alloy combinations and cermets can only be made by PM PM production can be automated for economical production

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Limitations and Disadvantages

High tooling and equipment costs

Metallic powders are expensive

Problems in storing and handling metal powders

Degradation over time, fire hazards with certain metals Limitations on part geometry because metal powders do not readily flow well Variations in density may be a problem, especially for complex geometries

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Production of Metallic Powders

Any metal can be made into powder form

Three principal methods by which metallic

powders are commercially produced 1.

Atomization

2.

Chemical

3.

Electrolytic

In addition, mechanical milling is occasionally used to reduce powder sizes

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High velocity gas stream flows through expansion nozzle, siphoning molten metal and spraying it into container

Gas Atomization Method

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Iron Powders for PM

Powders produced by water atomization

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Conventional Press and Sinter Steps

1.

Blending and mixing of powders

2.

Compaction - pressing into desired shape

3. Sintering - heating to temperature below melting point to cause solid 䇳state bonding of particles and strengthening of part

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Blending and Mixing of Powders

The starting powders must be homogenized

Blending - powders of the same chemistry but

possibly different particle sizes are intermingled Different particle sizes are often blended to reduce porosity

Mixing - powders of different chemistries are

combined

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Compaction

High pressure to form the powders into the required shape

Conventional compaction method is pressing, in

which opposing punches squeeze the powders contained in a die

The workpart after pressing is called a green

compact The green strength of the part should be adequate for handling

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Conventional Pressing in PM

Pressing in PM: (1) filling

die cavity with powder by automatic feeder; (2) initial and (3) final positions of upper and lower punches during pressing, (4) part ejection

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Sintering

Heat treatment to bond the metallic particles,

thereby increasing strength and hardness

Usually carried out at 70% to 90% of the

metal's melting point (absolute scale)

The primary driving force for sintering is

reduction of surface energy

Part shrinkage occurs during sintering due to

pore size reduction

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Sintering Sequence on a Microscopic Scale

(1) Particle bonding is initiated at contact points; (2) contact points grow into "necks"; (3) pores between particles are reduced in size; (4) grain boundaries develop between particles in place of necked regions

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(a) Typical heat treatment cycle in sintering; and (b) schematic cross section of a continuous sintering furnace

Sintering Cycle and Furnace

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Densification and Sizing

Secondary operations are performed on

sintered part to increase density, improve accuracy, or accomplish additional shaping

Repressing - pressing in closed die to increase

density and improve properties

Sizing - pressing to improve dimensional accuracy

Coining - pressing details into its surface

Machining - for geometric features that cannot be

formed by pressing, such as threads and side holes

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Impregnation and Infiltration

Porosity is a unique and inherent

characteristic of PM technology

It can be exploited to create special

products by filling the available pore space with oils, polymers, or metals

Two categories:

1.

Impregnation

2.

Infiltration

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Impregnation

The term used when oil or other fluid is

permeated into the pores of a sintered PM part

Common products are oil䇳impregnated

bearings, gears, and similar components Alternative application is when parts are impregnated with polymer resins that seep into the pore spaces in liquid form and then solidify to create a pressure tight part

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Infiltration

Operation in which the pores of the PM part are

filled with a molten metal

The melting point of the filler metal must be

below that of the PM part

Heating the filler metal in contact with the

sintered part so capillary action draws the filler into the pores

Resulting structure is nonporous, and the

infiltrated part has a more uniform density, as well as improved toughness and strength

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Alternative Pressing and Sintering Techniques

Some additional methods for producing PM

parts: Isostatic pressing - hydraulic pressure is applied from all directions to achieve compaction

Powder injection molding (PIM) - starting polymer

has 50% to 85% powder content

Polymer is removed and PM part is sintered

Hot pressing - combined pressing and sintering

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PM Materials - Elemental Powders

A pure metal in particulate form

Common elemental powders:

Iron

Aluminum

Copper

Elemental powders can be mixed with other

metal powders to produce alloys that are difficult to formulate by conventional methods

Example: tool steels

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Pre-Alloyed Powders

Each particle is an alloy comprised of the

desired chemical composition

Common pre-alloyed powders:

Stainless steels

Certain copper alloys

High speed steel

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PM Products

Gears, bearings, sprockets, fasteners,

electrical contacts, cutting tools, and various machinery parts

Advantage of PM: parts can be made to near

net shape or net shape

When produced in large quantities, gears and

bearings are ideal for PM because:

Their geometries are defined in two dimensions

There is a need for porosity in the part to serve as a reservoir for lubricant

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(a) Class I Simple thin shapes; (b) Class II Simple but thicker; (c) Class III Two levels of thickness; and (d)

Class IV Multiple levels of thickness

Four Classes of PM Parts

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Side Holes and Undercuts

Part features to be avoided in PM: (a) side

holes and (b) side undercuts since part ejection is impossible

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Design Guidelines

for PM Parts - III

Screw threads cannot be fabricated by PM

They must be machined into the part

Chamfers and corner radii are possible in PM

But problems occur in punch rigidity when angles

are too acute

Wall thickness should be a minimum of 1.5

mm (0.060 in) between holes or a hole and outside wall

Minimum hole diameter ~ 1.5 mm (0.060 in)

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Chamfers and Corner Radii

(a) Avoid acute angles; (b) use larger angles for punch rigidity; (c) inside radius is desirable; (d) avoid full outside corner radius because punch is fragile at edge; (e) better to combine radius and chamfer

NC State University

HW assignment

Reading assignment: Chapters, 20.4, 21

Review Questions: 10.1, 10.2, 10.3, 10.4, 10.5,

10.7, 10.8, 10.9, 10.11, 10.12, 10.14, 10.15,

Problems: 10.1,

Department of Materials Science and Engineering 27quotesdbs_dbs19.pdfusesText_25
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