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1. Baxter, C. S.; Garratt, P. J.; Vollhardt, K. P. C., The 3,4:5,6:9,10-

Tribenzobicyclo[6.2.0]decapentaenyl Dianion, J. Am. Chem. Soc. 1969, 91, 7783.

2. Garratt, P. J.; Vollhardt, K. P. C., Benzo[3,4]cyclobuta[1,2-c]thiophen (2-Thianorbiphenylene),

Chem. Commun. 1970, 109.

3. Garratt, P. J.; Vollhardt, K. P. C.; Mitchell, R. H., Wittig Reactions of 1,2-Dihydro-1,2-

bis(triphenylphosphoranylidene)benzocyclobutene and Benzocyclobutene-1,2-quinone. The Synthesis of Dibenzo[a,c]benzo[3,4]cyclobuta[1,2-f]cyclooctene, J. Chem. Soc. (C) 1970, 2137.

4. Garratt, P. J.; Holmes, A. B.; Sondheimer, F.; Vollhardt, K. P. C., The Synthesis of

Benzo[3,4]cyclobuta[1,2-e]dicyclohexeno[b,h]thionin, an Analog of Biphenylene Containing a

Thionin Ring, J. Am. Chem. Soc. 1970, 92, 4492.

5. Garratt, P. J.; Vollhardt, K. P. C., 6,11-Methanocyclobutabenzo[1,2-a]-[10]annulene, a

Biphenylene-ʌ-Electron Ring, Angew. Chem. 1971, 83, 111;

Angew. Chem., Int. Ed. Engl. 1971, 10, 125.

6. Garratt, P. J.; Vollhardt, K. P. C., Homophthalaldehyde, Synthesis 1971, 3, 423.

7. Garratt, P. J.; Holmes, A. B.; Sondheimer, F.; Vollhardt, K. P. C., The Synthesis of Mono-trans-

dicyclohexeno[b,i]-1,6-dithiacyclodeca-2,4,7,9-tetraene, a Tetra-alkylated 1,6-Dithia[10]annulene,

Chem. Commun. 1971, 947.

8. Garratt, P. J.; Vollhardt, K. P. C., Synthesis of Benzo[3,4]cyclobuta[1,2-a]benzo[d]tropylium

Cation, a Homobiphenylene Cation, Chem. Commun. 1971, 1143.

9. Garratt, P. J.; Vollhardt, K. P. C., The Synthesis of 6,7-Diphenyl-3-thiabicyclo[3.2.0]heptatriene,

a Thienocyclobutadiene, J. Am. Chem. Soc. 1972, 94, 1022.

10. Garratt, P. J.; Vollhardt, K. P. C., Wittig Reactions of 1,2-Benzocyclobutadienequinone.

Synthesis of 2-Thianorbiphenylene (Benzo-[3,4]cyclobuta[1,2-c]thiophene), J. Am. Chem. Soc.

1972, 94, 7087.

11. Vollhardt, K. P. C.; Bergman, R. G., 3,6-Dehydrooxepin, a Furocyclobutadiene, J. Am. Chem.

Soc. 1972, 94, 8950.

12. Jones, A. J.; Garratt, P. J.; Vollhardt, K. P. C., 13C Shifts in Biphenylene and Analogous

Compounds, Angew. Chem. 1973, 85, 260; Angew. Chem., Int. Ed. Engl. 1973, 12, 241.

14. Bergman, R. G.; Vollhardt, K. P. C., 3-Oxabicyclo[3,2,0]hepta-1,4-diene, Chem. Commun.

1973, 214.

15. Garratt, P. J.; Holmes, A. B.; Sondheimer, F.; Vollhardt, K. P. C., Wittig Reactions of 1,2-

Dihydro-1,2-bis(triphenylphosphoranylidene)benzocyclobutene. Synthesis of All-cis- and Mono- trans-1,2,3,4,6,7,8,9-octahydrodibenzo[b,h]benzo[3,4]cyclobuta-[1,2-e]thionin, Analogues of Biphenylene Containing a Thionin Ring, J. Chem. Soc., Perkin Trans. I 1973, 2253.

16. Vollhardt, K. P. C.; Bergman, R. G., Competition between Sulfur Extrusion and Thermal

Synthesis of Thienocyclobutadiene in the Pyrolysis of cis- and trans-1,2-Diethynylthiiranes. Dimerization of the Rearrangement Product to Bisthienocyclooctatetraene, J. Am. Chem. Soc.

1973, 95, 7538.

17. Vollhardt, K. P. C.; Bergman, R. G., A One-Step Synthesis of Benzocyclobutenes Involving

Cooligomerization of Linear Mono- Ș5-Cyclopentadienylcobalt

Dicarbonyl, J. Am. Chem. Soc. 1974, 96, 4996.

18. Vollhardt, K. P. C.; Bercaw, J. E.; Bergman, R. G., Isolation of Unstable Bis(Ș5-

cyclopentadienylcobalt) Tricarbonyl from the Irradiation of Ș5-Cyclopentadienylcobalt Dicarbonyl. Thermal Reactions of this Binuclear Complex Leading to Starting Material and Trinuclear and Tetranuclear Cobalt (I) Complexes, J. Am. Chem. Soc. 1974, 96, 4998.

19. Vollhardt, K. P. C., Bis-Wittig Reactions in the Synthesis of Nonbenzenoid Aromatic Ring

Systems, Synthesis 1975, 7, 765.

20. Vollhardt, K. P. C., Cyclobutadienoids, Top. Curr. Chem. 1975, 59, 113.

21. Aalbersberg, W. G. L.; Barkovich, A. J.; Funk, R. L.; Hillard III, R. L.; Vollhardt, K. P. C.,

Transition Metal Catalyzed Acetylene Cyclizations. 4,5-Bis(trimethylsilyl)benzocyclobutene, a Highly Strained, Versatile Synthetic Intermediate, J. Am. Chem. Soc. 1975, 97, 5600.

22. Vollhardt, K. P. C.; Bercaw, J. E.; Bergman, R. G., Photochemistry of Ș5-

Cyclopentadienylcobalt Dicarbonyl and Thermal Decomposition of Derived Cobalt Cluster

Complexes. Isolation of Bis(Ș5-cyclopentadienylcobalt) Tricarbonyl, Tris(Ș5-cyclopentadienylcobalt

Monocarbonyl) and Tetra(Ș5-Cyclopentadienylcobalt) Dicarbonyl, J. Organomet. Chem. 1975, 97, 283.

23. Hillard III, R. L.; Vollhardt, K. P. C., Transition Metal Catalyzed Acetylene Cyclizations. A

General Synthesis of Indans and Tetralins, Angew. Chem. 1975, 87, 744; Angew. Chem., Int. Ed.

Engl. 1975, 14, 712.

24. Brogli, F.; Heilbronner, E.; Wirz, J.; Kloster-Jensen, E.; Bergman, R. G.; Vollhardt, K. P. C.;

ıʌ-, Di- and

Triacetylenes. A Photoelectron Spectroscopic Investigation, Helv. Chim. Acta 1975, 58, 2620.

25. Saward, C. J.; Vollhardt, K. P. C., 1,2-Cyclopropa-4,5-cyclobutabenzene, a Novel Strained

Benzene Derivative, Tetrahedron Lett. 1975, 4539.

26. Funk, R. L.; Vollhardt, K. P. C., 10,11-Dihydrocyclobuta[b]triphenylene and 1,2,5,6,9,10-

Hexahydrotriscyclobuta[b,h,n]triphenylene, Angew. Chem. 1976, 88, 63; Angew. Chem., Int. Ed.

Engl. 1976, 15, 53.

27. Barkovich, A. J.; Vollhardt, K. P. C., 1,5,9-Cyclododecatriyne. Synthesis and Conversion to

Intermediate 1,2:3,4:5,6-Tricyclobutabenzene, J. Am. Chem. Soc. 1976, 98, 2667.

28. Hillard III, R. L.; Vollhardt, K. P. C., Cyclobuta[1,2-d]benzyne. Generation, Trapping, and

Dimerization to 2,3:6,7-Dicyclobutabiphenylene, J. Am. Chem. Soc. 1976, 98, 3579.

29. Funk, R. L.; Vollhardt, K. P. C., Hexa-1,5-diyn-3-ol Ethers as Tetramethynyl Synthons in

Cobalt-catalysed Acetylene Co-oligomerisations; A One Step Synthesis of 2,3,6,7- Tetrakistrimethylsilylnaphthalene, J. Chem. Soc., Chem. Commun. 1976, 833.

30. Funk, R. L.; Vollhardt, K. P. C., In Situ Generation and Intramolecular Trapping of o-Xylylenes

by Cobalt-Catalyzed Acetylene Cooligomerizations. A One-Step Synthesis of Polycycles, J. Am.

Chem. Soc. 1976, 98, 6755.

31. Vollhardt, K. P. C., Transition-Metal-Catalyzed Acetylene Cyclizations in Organic Synthesis,

Acc. Chem. Res. 1977, 10, 1.

32. Vollhardt, K. P. C.; Lee, L. S., 1,2-ʌ-

Electron System, J. Am. Chem. Soc. 1977, 99, 2010.

33. Aalbersberg, W. G. L.; Vollhardt, K. P. C., Retention of Stereochemistry in the Extrusion of

Sulfur Monoxide from Thiirane Oxides. Synthesis and Thermal Decomposition of cis-and trans- Dideuteriothiirane Oxide, J. Am. Chem. Soc. 1977, 99, 2792.

34. Hillard III, R. L.; Vollhardt, K. P. C., Substituted Benzocyclobutenes, Indans, and Tetralins via

Cobalt-ĮȦ-Diynes with Substituted Acetylenes. Formation and Synthetic Utility of Trimethylsilylated Benzocycloalkenes, J. Am. Chem. Soc. 1977, 99, 4058.

35. Hillard III, R. L.; Vollhardt, K. P. C., 3,4-Bis(trimethylsilyl)benzocyclobutene - Synthesis by

Acetylene Cotrimerization and Conversion into 1,2-Dihydrocyclobuta[c]benzyne, Angew. Chem.

1977, 89, 413; Angew. Chem., Int. Ed. Engl. 1977, 16, 399.

36. Naiman, A.; Vollhardt, K. P. C., A Cobalt-Catalyzed One-Step Synthesis of Annulated

Pyridines, Angew. Chem. 1977, 89, 758; Angew. Chem., Int. Ed. Engl. 1977, 16, 708.

37. Funk, R. L.; Vollhardt, K. P. C., A Cobalt-Catalyzed Steroid Synthesis, J. Am. Chem. Soc.

1977, 99, 5483.

38. Vollhardt, K. P. C., Cobaltkatalysierte Acetylen-Cyclisierungen, Nachr. Chem. Tech. 1977, 25,

584.

39. Barkovich, A. J.; Strauss, E. S.; Vollhardt, K. P. C., Hexaradialene, J. Am. Chem. Soc. 1977,

99, 8321.

40. Fritch, J. R.; Vollhardt, K. P. C., Bicyclobutadienylene (tricyclo-[4.2.0.02,5]octa-1,2,5,7-

tetraene)-Ș5-cyclopentadienylcobalt. A Possible Intermediate in the Remarkable Gas Phase Rearrangement of 1,2-Diethynyl-Ș4-cyclobutadiene-Ș5-cyclopentadienylcobalt, J. Am. Chem. Soc.

1978, 100, 3643.

41. Vollhardt, K. P. C., Transition Metal Catalyzed Acetylene Cooligomerizations for the Synthesis

of Complex Molecules, The Strem Chemiker 1978, 6(2), 1.

42. Perkins, P.; Vollhardt, K. P. C., 1,2,8,9-Tetrahydrodicyclobuta[b,g]phenanthrene and 1,2,7,8-

Tetrahydrodicyclobuta[b,h]phenanthrene, Potentially Carcinogenic Activated Hydrocarbons, Angew. Chem. 1978, 90, 643; Angew. Chem., Int. Ed. Engl. 1978, 17, 615.

43. Fritch, J. R.; Vollhardt, K. P. C., Cyclobutadiene-Metal Complexes as Potential Intermediates

in Alkyne Metathesis: Flash Vacuum Pyrolysis of Substituted Ș4-Cyclobutadiene-Ș5- cyclopentadienylcobalt Complexes, Angew. Chem. 1979, 91, 439; Angew. Chem., Int. Ed. Engl.

1979, 18, 409.

44. Funk, R. L.; Vollhardt, K. P. C., The Cobalt Way to dl-Estrone, a Highly Regiospecific

Functionalization of 2,3-Bis(trimethylsilyl)estratriene-17-one, J. Am. Chem. Soc. 1979, 101, 215.

45. Duclos, R. I.; Vollhardt, K. P. C.; Yee, L. S., Ș4-Benzocyclobutadiene-Ș5-

cyclopentadienylcobalt, A New "Aromatic" Sandwich Complex, J. Organomet. Chem. 1979, 174, 109.

46. Fritch, J. R.; Vollhardt, K. P. C.; Thompson, M. R.; Day, V. W., Apparent Concurrent

Acetylene-Vinylidenecarbene Rearrangements, Silyl-Acetylide Metathesis, and Alkyne Cleavage in the Interaction of Bis(trimethylsilyl)acetylene with (Ș5-C5H5)Co(CO)2 Crystal and Molecular

Structure of a Novel Biscarbyne Complex: [3Ș1-CSi(CH3)3][3Ș1-C3Si(CH3)3][(Ș5-C5H5)Co]3, J. Am.

Chem. Soc. 1979, 101, 2768.

47. Müller, C.; Schweig, A.; Thiel, W.; Grahn, W.; Vollhardt, K. P. C.; Bergman, R. G.,

Photoelectron Spectra of 2,5-Dehydrotropylidene, 3,6-Dehydrooxepin, and Fulvenallene, J. Am.

Chem. Soc. 1979, 101, 5579.

48. Aalbersberg, W. G. L.; Vollhardt, K. P. C., Intramolecular Cycloadditions of Bis-o-Xylylenes.

An Extremely Short Route to [2.2.2]Cyclophanes, Tetrahedron Lett. 1979, 1939.

49. Vollhardt, K. P. C., Anwendungen von Übergangsmetallen in der Organischen Synthese:

Faszinierende Neuartige Synthesewege in der Konstruktion Komplexer Moleküle, Chem. Ztg.

1979, 103, 309.

50. Vollhardt, K. P. C., Transition Metal Mediated Transformations in the Synthesis of Complex

Molecules, MMRD-Newsletter 1979, 3(1), 1.

51. Houk, K. N.; Strozier, R. W.; Santiago, C.; Gandour, R. W.; Vollhardt, K. P. C., Electronic

Structure and Photoelectron Spectrum of 1,5,9-Cyclododecatriyne, J. Am. Chem. Soc. 1979, 101, 5183.

52. Naiman, A.; Vollhardt, K. P. C., 1,2,4,5-Tetrahydrodicyclobuta[b,e]pyridine, Angew. Chem.

1979, 91, 440; Angew. Chem., Int. Ed. Engl. 1979, 18, 411.

53. Perkins, P.; Vollhardt, K. P. C., Polymer-Supported Ș5-Cyclopentadienylcobalt. An

Immobilized "Homogeneous" Fischer-Tropsch Catalyst, J. Am. Chem. Soc. 1979, 101, 3985.

54. Vollhardt, K. P. C., The Cobalt Way to Estrone, Lecture published in the Proceedings of the

26th National Organic Symposium, Tucson, Arizona, 1979, 105.

55. Vollhardt, K. P. C., The Cobalt Way to Estrone, Ann. N.Y. Acad. Sci. 1980, 333, 241.

56. Barkovich, A. J.; Strauss, E. S.; Vollhardt, K. P. C., Unusual Rearrangements in the C12H12-

Manifold: 1,5,9-Cyclododecatriyne, 1,2:3,4:5,6-Tricyclobutabenzene, Hexaradialene, Isr. J. Chem.

1980, 20, 225.

57. Funk, R. L.; Vollhardt, K. P. C., Thermal, Photochemical, and Transition-Metal Mediated

Routes to Steroids by Intramolecular Diels-Alder Reactions of o-Xylylenes (o-Quinodimethanes),

Chem. Soc. Rev. 1980, 9, 41.

58. Vollhardt, K. P. C., Physical, Chemical, and Some Biological Properties of Strained Ring

Hydrocarbons, Pure Appl. Chem. 1980, 52, 1645.

59. Funk, R. L.; Vollhardt, K. P. C., 2-Methyl-2-cyclopenten-1-one from 2-Methylcyclopentane-

1,3-dione, Synthesis, 1980, 12, 118.

60. Hillard III, R. L.; Vollhardt, K. P. C., Potential Routes to Cyclobuta[1,2-c] Cyclopropabenzene,

Tetrahedron, 1980, 36, 2435.

61. Fritch, J. R.; Vollhardt, K. P. C., Biscarbyne Clusters by Alkyne Cleavage: A General Reaction,

Angew. Chem. 1980, 92, 570; Angew. Chem., Int. Ed. Engl. 1980, 19, 559.

62. Funk, R. L.; Vollhardt, K. P. C., Cooligomerizations of 3-Substituted 1,5-Hexadiynes With

Bis(trimethylsily)acetylene Catalyzed by Cobalt. A General Synthesis of Tricyclic Ring Systems From Acyclic Precursors, J. Am. Chem. Soc. 1980, 102, 5245.

63. Funk, R. L.; Vollhardt, K. P. C., Transition-Metal-Catalyzed Alkyne Cyclizations, A Cobalt-

Mediated Total Synthesis of dl-Estrone, J. Am. Chem. Soc. 1980, 102, 5253.

64. Gesing, E. R. F.; Sinclair, J. A.; Vollhardt, K. P. C., 1,3-Bis(trimethylsilyl)propyne and

Alkyltrimethylsilylalkynes as Efficient Co-oligomerisation Partners in Cobalt-catalysed Alkyne Cyclisations, J. Chem. Soc., Chem. Commun. 1980, 286.

65. Sternberg, E. D.; Vollhardt, K. P. C., Cobalt-Mediated Cyclizations of Linear Achiral Diynenes.

A One-Step Construction of Complexed Chiral Polycycles, J. Am. Chem. Soc. 1980, 102, 4839.

66. Gesing, E. R. F.; Tane, J. P.; Vollhardt, K. P. C., Cobalt Mediated [2+2+2]-Cycloadditions: A

Simple Route to Substituted Cyclopentadienones, Angew. Chem. 1980, 92, 1057; Angew. Chem.,

Int. Ed. Engl. 1980, 19, 1023

67. K. P. C. Vollhardt and R. L. Funk, Cobalt Catalyzed Steroid Synthesis, US 4183864

19800115, January 15, 1980.

68. K. P. C. Vollhardt and P. Perkins, Fischer-Tropsch Catalysts, US 39986 19800912, October

28, 1980.

69. Chang, C.; Francisco, C. G.; Gadek, T. R.; King Jr., J. A.; Sternberg, E. D.; Vollhardt, K. P. C.,

Transition Metal Mediated Carbon-Carbon Bond Formations. A General, Partially Chemo-, Regio-, and Stereospecific Synthesis of Annelated Cyclohexadienes From Acyclic Starting Materials, in Organic Synthesis Today and Tomorrow (IUPAC); Trost, B.M. and Hutchinson, C. R., Eds.;

Pergamon Press: New York, 1981; p. 71.

70. Ville, G.; Vollhardt, K. P. C.; Winter, M. J., On the Reversibility of Ș4-Cyclobutadiene-Metal

Formation from Complexed Alkynes: Unimolecular Isomerization of Labeled Racemic and Enantiomerically Enriched Ș5-Cyclopentadienyl-Ș4-cyclobutadiene-Cobalt Complexes, J. Am.

Chem. Soc. 1981, 103, 5267.

71. Huggins, J. M.; King Jr., J. A.; Vollhardt, K. P. C., Winter, M. J., Separation of Diastereomers,

Structural Isomers, and Homologs of Ș5-Cyclopentadienylcobalt and Dinuclear Molybdenum Complexes by Reverse Phase High Performance Liquid Chromatography Using Deoxygenated

Solvents, J. Organomet. Chem. 1981, 208, 73.

72. Benner, L. S.; Perkins, P.; Vollhardt, K. P. C., Hydrocarbon Formation on Polymer-Supported

Ș5-Cyclopentadienyl Cobalt, ACS Symp. Ser. 1981, 152, 165.

73. Chang, C.-A.; King Jr., J. A.; Vollhardt, K. P. C., Intermolecular Cobalt-mediated

[2+2+2]Cyclo-additions: Regiospecific One-ĮȦ-Enynes and Alkynes, J. Chem. Soc., Chem. Commun. 1981, 53.

74. Aalbersberg, W. G. L.; Vollhardt, K. P. C., The Nature of Sulfur Monoxide From Thiirane

Oxide: A Stereochemical Test, Isr. J. Chem. 1981, 21, 145.

75. Lai, Y-H.; Tam, W.; Vollhardt, K. P. C., ʌ-Complexed Benzene:

Double Nucleophilic Addition, J. Organomet. Chem. 1981, 216, 97.

76. Gesing, E. R. F.; Vollhardt, K. P. C., The Variety of Compounds From the Interaction of 1,5-

Diynes with Ș5-Cyclopentadienyl Cobalt: 1,6-Bis(trimethylsilyl)-1,5-hexadiyne, a Complete Product Analysis, J. Organomet. Chem. 1981, 217, 105.

77. Gadek, T. R.; Vollhardt, K. P. C., Cobalt Mediated [2+2+2]-Cycloadditions: Stereospecific

Intramolecular Reactions of Enediynes to Tricyclic Dienes Bearing Angular Methyl Groups, Angew. Chem. 1981, 93, 801; Angew. Chem., Int. Ed. Engl. 1981, 20, 802.

78. Benner, L. S.; Lai, Y-H.; Vollhardt, K. P. C., On the Purported Fischer-Tropsch Alkylation of

Benzene: Reaction of Benzene With Aluminum Trichloride Revisited, J. Am. Chem. Soc. 1981,

103, 3609.

79. Colborn, R. E.; Vollhardt, K. P. C., Mechanism of the Reppe Cyclooctatetraene Synthesis

From Ethyne: A Labeling Experiment, J. Am. Chem. Soc. 1981, 103, 6259.

80. Ville, G.; Vollhardt, K. P. C., Carbon-Carbon and Carbon-Hydrogen Coupling Constants in

Neutral Coordinated Cyclobutadienes, J. Magn. Res. 1981, 45, 525.

81. Vollhardt, K. P. C., Cobalt Mediated Bond Forming and Bond Breaking Reactions: Synthetic

and Mechanistic Perambulations, Chem. Aust. 1982, 49, 1.

82. Fritch, J. R.; Vollhardt, K. P. C., The Diethynylcyclobutadiene Rearrangement: A Degenerate

Ligand Reorganization in the Coordination Sphere of (Ș5-Cyclopentadienyl)cobalt,

Organometallics 1982, 1, 590.

83. Van Horn, D. E.; Vollhardt, K. P. C., Some Remarkable Reactions of the Biscarbyne Clusters

[ȝ3-(Ș1-CR1)-ȝ3-(Ș1-CR2)-{(Ș5-C5H5)Co}3] With Electrophiles, J. Chem. Soc., Chem. Commun.

1982, 203.

84. Brien, D. J.; Naiman, A.; Vollhardt, K. P. C., Catalytic Co-ĮȦ-Cyanoalkynes

with Alkynes: a Versatile Chemo- and Regio-selective Synthesis of 2,3-Substituted 5,6,7,8- Tetrahydroquinolines and Other Cycloalka[1,2-b]pyridines, J. Chem. Soc., Chem. Commun. 1982, 133.

85. Berris, B. C.; Vollhardt, K. P. C., An Approach to Tricyclo[8.4.0.04,7]Tetradecahepta-

1,3,5,7,9,11,13-ene (Benzo[1,2-a]cyclobuta [1,2-e]cyclooctatetraene): Unusual Thermal

Rearrangements in the C14H10-Manifold, Tetrahedron 1982, 38, 2911.

86. Earl, R. A.; Vollhardt, K. P. C., On the Synthetic Utility of Thermally Generated Imines: The

Retro-ene Imino Diels-Alder Reaction, Heterocycles 1982, 19, 265.

87. Sternberg, E. D.; Vollhardt, K. P. C., Cobalt-Mediated [2+2+2] Cycloadditions En Route to

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